This unique book is the Proceedings of the 8th International Symposium on the Characterisation of Porous Solids, known also as "COPS VIII". The conference is one of a series, held every three years, which covers developments in methods for the characterisation of porous materials, and applications of those methods. The scope of the conference: COPS VIII is concerned with fundamental and applied research on the characterisation of the structure of porous materials, and the relationship between structure and material performance. The scope includes experimental characterisation methods such as X-Ray diffraction, NMR, adsorption, mercury intrusion, and calorimetry; theoretical and simulation methods used to interpret experimental data, such as molecular simulation, classical and statistical mechanical theory, and pore network modelling; and applied research on the impact of measured material properties on performance in applications.

This book contains 99 of the papers that were presented at the 6th in the series of Symposia on Characterization of Porous Solids held in Alicante, Spain, May 2002. Written by leading international specialists in the subject, the contributions represent an up-to-date and authoritative account of recent developments around the world in the major methods used to characterize porous solids. The book is a useful work of reference for anyone interested in characterizing porous solids, such as MCM-41 mesoporous materials, pillared clays, etc. Papers on pore structure determination using gas adsorption feature strongly, together with papers on small angle scattering methods, mercury porosimetry, microcalorimetry, scanning probe microscopies, and image analysis.

The declared objective of this book is to provide an introductory review of the various theoretical and practical aspects of adsorption by powders and porous solids with particular reference to materials of technological importance. The primary aim is to meet the needs of students and non-specialists who are new to surface science or who wish to use the advanced techniques now available for the determination of surface area, pore size and surface characterization. In addition, a critical account is given of recent work on the adsorptive properties of activated carbons, oxides, clays and zeolites. - Provides a comprehensive treatment of adsorption at both the gas/solid interface and the liquid/solid interface - Includes chapters dealing with experimental methodology and the interpretation of adsorption data obtained with porous oxides, carbons and zeolites - Techniques capture the importance of heterogeneous catalysis, chemical engineering and the production of pigments, cements, agrochemicals, and pharmaceuticals

The objectives of the Third IUPAC Symposium on the Characterization of Porous Solids (COPS-III) were (1) to provide the opportunity for specialists to exchange ideas and new information on theoretical principles and methodology and (2) to generate proposals for the comparison and utilization of the many techniques now available for the characterization of porous solids. A successful outcome of the Symposium has been the final report of the IUPAC Subcommittee on Recommendations for the Characterization of Porous Solids, a summary of which is given in these proceedings. The edited papers included in the present volume have been selected from the 155 oral and poster presentations given at this symposium, which attracted 200 participants from 28 different countries. The following topics were discussed:1. Simulation and modelling of pore structures and pore-filling mechanisms2. Novel experimental techniques with particular reference to high-resolution techniques3. Model pore structures and reference materials4. Porous materials of technological importance.The wide range of materials and techniques described provide a useful and comprehensive reference source for academic and industrial scientists and technologists.

This book provides authoritative information, techniques and data necessary for the appropriate understanding of biomass and biowaste (understood as contaminated biomass) composition and behaviour while processed in various conditions and technologies. Numerous techniques for characterizing biomass, biowaste and by-product streams exist in literature. However, there lacks a reference book where these techniques are gathered in a single book, although such information is in increasingly high demand. This handbook provides a wealth of characterization methods, protocols, standards, databases and references relevant to various biomass, biowaste materials and by-products. It specifically addresses sampling and preconditioning methods, extraction techniques of elements and molecules, as well as biochemical, mechanical and thermal characterization methods. Furthermore, advanced and innovative methods under development are highlighted. The characterization will allow the analysis, identification and quantification of molecules and species including biomass feedstocks and related conversion products. The characterization will also provide insight into physical, mechanical and thermal properties of biomass and biowaste as well as the resulting by-products.

The growth of interest in newly developed porous materials has prompted the writing of this book for those who have the need to make meaningful measurements without the benefit of years of experience. One might consider this new book as the 4th edition of "Powder Surface Area and Porosity" (Lowell & Shields), but for this new edition we set out to incorporate recent developments in the understanding of fluids in many types of porous materials, not just powders. Based on this, we felt that it would be prudent to change the title to "Characterization of Porous Solids and Powders: Surface Area, Porosity and Density". This book gives a unique overview of principles associated with the characterization of solids with regard to their surface area, pore size, pore volume and density. It covers methods based on gas adsorption (both physi and chemisorption), mercury porosimetry and pycnometry. Not only are the theoretical and experimental basics of these techniques presented in detail but also, in light of the tremendous progress made in recent years in materials science and nanotechnology, the most recent developments are described. In particular, the application of classical theories and methods for pore size analysis are contrasted with the most advanced microscopic theories based on statistical mechanics (e.g. Density Functional Theory and Molecular Simulation). The characterization of heterogeneous catalysts is more prominent than in earlier editions; the sections on mercury porosimetry and particularly chemisorption have been updated and greatly expanded.

Calorimetric Methods for the Characterization of Porous Materials presents calorimetric methods used in the characterization of porous materials using chemical thermodynamics. Among these materials, catalysts, supports and adsorbents (such as Activated Carbon, Metal-Organic-Frameworks, SBA-15, Zeolites, Graphene, Graphite, Carbon Foams) are presented. In addition, the use of calorimetry in the study of catalytic reactions in different phases is explored—applicable to air and wastewater treatment, clean and renewable energies, green chemistry, as well as energy production and storage (Carbon dioxide, methane and hydrogen at high pressure). Chapters summarize basic concepts of thermodynamics and kinetics alongside experimental techniques such as thermal analysis and calorimetry. In addition, information is given about different calorimetric methods that can be used in studies aimed at characterizing the physicochemical properties of adsorbents, supports and solid catalysts, as well as the processes related to the adsorption-desorption phenomena of the reactants and/or products of catalytic reactions. - Addresses the problems involved with the chemical thermodynamics of porous materials, with a significant practical element explaining experimental parameters and how to perform calculations - Presents, in detail, the main instrumental calorimetric methods, including those that must be carefully considered to avoid experimental errors - Demonstrates, step-by-step, how to perform calculations using data obtained from instrumentation to achieve reliable results - Provides novel explanations on how to use calorimetry in catalyst characterization - Allows readers to broaden the spectrum of the application of calorimetry in the study of materials

The problem of storing hydrogen safely and effectively is one of the major technological barriers currently preventing the widespread adoption of hydrogen as an energy carrier and the subsequent transition to a so-called hydrogen economy. Practical issues with the storage of hydrogen in both gas and liquid form appear to make reversible solid state hydrogen storage the most promising potential solution. Hydrogen Storage Materials addresses the characterisation of the hydrogen storage properties of the materials that are currently being considered for this purpose. The background to the topic is introduced, along with the various types of materials that are currently under investigation, including nanostructured interstitial and complex hydrides, and porous materials, such as metal-organic frameworks and microporous organic polymers. The main features of Hydrogen Storage Materials include: an overview of the different types of hydrogen storage materials and the properties that are of interest for their practical use; descriptions of the gas sorption measurement methods used to determine these properties, and the complementary techniques that can be used to help corroborate hydrogen uptake data; and extensive coverage of the practical considerations for accurate hydrogen sorption measurement that drive both instrument design and the development of experimental methodology. Hydrogen Storage Materials provides an up-to-date overview of the topic for experienced researchers, while including enough introductory material to serve as a useful, practical introduction for newcomers to the field.

This volume contains a collection of 19 papers from the 11th International Symposium on Ceramic Materials and Components for Energy and Environmental Applications (CMCEE-11), June 14-19, 2015 in Vancouver, BC, Canada. Papers were presented in the below five symposia from Track 2 on the topic of Ceramics for Energy Conservation and Efficiency: Advanced Ceramics and Composites for Gas Turbine Engines Advanced Refractory Ceramic Materials and Technologies Advanced Ceramic Coatings for Power Systems Energy Efficient Advanced Bearings and Wear Resistant Materials Advanced Nitrides and Related Materials for Energy Applications

Material and contact characterisation is a rapidly advancing field that requires the application of a combination of numerical and experimental methods. Including papers from the International Conference on Computational Methods and Experiments in Material and Contact Characterisation this volume presents the latest research in the field.