The aim of this book is to familiarize the reader with the practical aspects of polymer analysis. A wealth of practical detail, including some detailed methods is included. The book covers not only the analysis of the main types of polymers and copolymers now in use commercially, but also the analysis of minor non-polymeric components of the polymer formulation, whether they be deliberately added, such as processing additives, or whether they occur adventitiously, such as moisture and residual monomers and solvent. A broad scheme for the examination of polymers is discussed in Chapter 2. Practically all of the major newer analytical techniques and many of the older classical techniques, have been used to examine polymers and their additive systems. As so many different polymers are now used commercially it is also advisable when attempting to identify a polymer to classify it by first separating it into pure polymeric and gross non polymeric fractions (Chapter Z) and then carrying out at least a qualitative elemental analysis and possible a quantitative analysis (Chapters 3 and 4) and then in some cases, depending on the elements found, to carry out functional group analysis (Chapters 6 and 9).

Ein Praxisleitfaden der Polymeranalyse für alle, die sich in Polymerlabors mit Analytik, Qualitätskontrolle oder Produktentwicklung beschäftigen. Der Autor erläutert, aus seinem umfangreichen Erfahrungsschatz, welche Probleme in welchen Situationen auftreten können. Viele Fallstudien helfen bei der Anwendung der Erkenntnisse im Laboralltag. Mit einer umfangreichen Datensammlung zu physikalischen Eigenschaften von Polymeren! (07/00)

This industrially relevant resource covers all established and emerging analytical methods for the deformulation of polymeric materials, with emphasis on the non-polymeric components. Each technique is evaluated on its technical and industrial merits. Emphasis is on understanding (principles and characteristics) and industrial applicability. Extensively illustrated throughout with over 200 figures, 400 tables, and 3,000 references.

This revolutionary and best-selling resource contains more than 200 pages of additional information and expanded discussions on zeolites, bitumen, conducting polymers, polymerization reactors, dendrites, self-assembling nanomaterials, atomic force microscopy, and polymer processing. This exceptional text offers extensive listings of laboratory exercises and demonstrations, web resources, and new applications for in-depth analysis of synthetic, natural, organometallic, and inorganic polymers. Special sections discuss human genome and protonics, recycling codes and solid waste, optical fibers, self-assembly, combinatorial chemistry, and smart and conductive materials.

Since the introduction of FT-NMR spectroscopy around five decades ago, NMR has achieved significant advances in hardware and methodologies, accompanied with the enhancement of spectral resolution and signal sensitivity. Rapid developments in the polymers field mean that accurate and quantitative characterization of polymer structures and dynamics is the keystone for precisely regulating and controlling the physical and chemical properties of the polymer. This book specifically focuses on NMR investigation of complex polymers for the polymer community as well as NMR spectroscopists, and will push the development of both fields. It covers the latest advances, for example high field DNP and ultrafast MAS methodologies, and show how these novel NMR methods characterize various synthetic and natural polymers.

Analytical Pyrolysis of Synthetic Organic Polymers is a follow-up to Analytical Pyrolysis of Natural Organic Polymers, which is volume 20 of the series. The main focus of the book is on practical applications of analytical pyrolysis in synthetic organic polymer identification and characterization. The first part of the book has five chapters including an introduction, a discussion on physico-chemistry of thermal degradation of synthetic polymers and on instrumentation used in analytical pyrolysis, a chapter discussing what type of information can be obtained from analytical pyrolysis, and a chapter dedicated to the analysis and characterization of synthetic polymers.The second part systematically covers the analytical pyrolysis of various classes of synthetic polymers. Some theoretical background for the understanding of polymer structure using analytical pyrolysis is also discussed.* Includes broad coverage of organic synthetic macromolecules* Focuses on physico-chemistry of thermal degradation, and the analytical pyrolysis of various classes of synthetic polymers* Is well written and suitable for both researchers and chemists working in analytical chemistry or in synthetic polymers

Based on Wiley's renowned Encyclopedia of Polymer Science and Technology, this book provides coverage of key methods of characterization of the physical and chemical properties of polymers, including atomic force microscopy, chromatographic methods, laser light scattering, nuclear magnetic resonance, and thermal analysis, among others. Written by prominent scholars from around the world, this reference presents over twenty-five self -contained articles on the most used analytical techniques currently practiced in polymer science.

Emphasis is on a broad description of the general methods and processes for the synthesis, modification and characterization of macromolecules. These more fundamental chapters will be supplemented by selected and detailed experiments. In addition to the preparative aspects, the book also gives the reader an impression on the relation of chemical constitution and morphology of Polymers to their properties, as well as on their application areas. Thus, an additional textbook will not be needed in order to understand the experiments. The 5th edition contains numerous changes: In recent years, so-called functional polymers which have special electrical, electronic, optical and biological properties, have gained more and more in interest. This textbook was therefore supplemented by recipes which describe the synthesis of these materials in a new chapter "Functional polymers". Together with new experiments in chapter 3,4 and 5 the book now contains more than 120 recipes that describe a wide range of macromolecules. From the reviews of recent editions: "This is an excellent book for all polymer chemists engaged in synthesis research studies and education. It is educationally sound and has excellent laboratory synthetic examples. The fundamentals are well done for the teaching of students and references are resonably up-to-date. As in previous issues, there are sections dealing with an introduction; structure and nomenclature; methods and techniques for synthesis, characterization, processing and modification of polymers. ....The authors have noted the following changes from previous editions- a new section on correlations of structure, morphology and properties; revision and enlargement of other property and characterization procedures; additional new experiments such as controlled radical polymerization; enzymatic polymerizations; microelmulsions; and electrical conducting polymers. This is a high quality textbook at a reasonable price and should be considered as a suitable reference for all engaged in synthetic areas of polymer research." (Eli M. Pearce, Polytechnic University, Brooklyn, NY, USA)

The selection and application of engineered materials is an integrated process that requires an understanding of the interaction between materials properties, manufacturing characteristics, design considerations, and the total life cycle of the product. This reference book on engineering plastics provides practical and comprehensive coverage on how the performance of plastics is characterized during design, property testing, and failure analysis. The fundamental structure and properties of plastics are reviewed for general reference, and detailed articles describe the important design factors, properties, and failure mechanisms of plastics. The effects of composition, processing, and structure are detailed in articles on the physical, chemical, thermal, and mechanical properties. Other articles cover failure mechanisms such as: crazing and fracture; impact loading; fatigue failure; wear failures, moisture related failure; organic chemical related failure; photolytic degradation; and microbial degradation. Characterization of plastics in failure analysis is described with additional articles on analysis of structure, surface analysis, and fractography.